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By J R Hanson; R B Boar; Royal Society of Chemistry.; et al

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R. Hanson, J. Chem. ,Perkin Trans. 1, 1980, 741. A. P. W. Bradshaw and J. R. Hanson, J. Chem. ,Chem. , 1979,924. 120 T . Murakami, T. Satake, K. Ninomiya, H. Iida, K. Yamauchi, N. Tanaka, Y. -M. Chen, Phytochemistry, 1980, 19, 1743. 12' W. A. Ayer and R. H. , 1980, 21, 1917. 122 W. A. Ayer and R. H. , 1980, 21, 1921. Sesquiterpenoids 41 CH20H GlucO HO OH OH (271) (270) H02C* OH (272) * R (273) R (2741 R = = H OH \ OH OH (276) R (277) R (278) R = = = C1 OGluc OAllosyl (279) R' (280) R' (281) R' = = = CH20H, R2 = Me Me,R2 = CH20H C02H, R2 = Me A full report on the synthesis of dihydrofomannosin acetate (284) has been p ~ b l i s h e d .

Darias, J. D. Martin, V. S. Martin, M. Norte, C. PCrez, A. Perales, and J. , 1980,21, 1151. A. Perales, M. Martinez-Ripoll, and J. , 1979,B35,2771. Suzuki, Chem. , 1980,541. " It co-occurs with aplysin (1 17), debromoaplysin (1 16), pacifenol(168), 79 M. Suzuki, N. Kowata, and E. Kurosawa, Tetrahedron, 1980,36, 1551. S. J. Selover and P. Crews, J. Org. , 1980,45, 69. 26 Terpenoids and Steroids and pacifidiene (172). Kylinone (171) can be obtained by treatment of deoxyprepacifenol (173) with boron trifluoride etherate, thus suggesting a biogenetic link between the two compounds.

D. Hernandez, Z. Taira, and W. H. Watson, Tetrahedron, 1980,36, 731. L. Piovetti, G. Combaut, and A. Diara, Phytochemistry, 1980, 19,2117. 86 Previously these two compounds have been converted into (+)-zizaene (189). 0'*5]undecyl skeleton involves the intramolecular 1 iii-v, - - 0 vi, vii viii-x PhS* i PhS' OTs 1 x i . SMe,; ix, H,O,-OH-; x, TsCI-py ; xi, MCPBA; xii, KOBu'; xiii, Na-Hg-Na2HP04; xiv, (CO,H),-H,O; xv, NaOMe Scheme 22 " 86 L. Piovetti and A . Diara, Phytochemistry, 1977, 16, 103; L.

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